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Conjugation Service by Types

Service by Molecules

Bioconjugation Selection
Oligo, Nucleic Acids
Peptide, Amino Acids
Protein Bioconjugation
Antibody, AB Fragments
Enzyme Bioconjugation
Reporter Molecule Labeling
Glycoconjugation
Liposome Bioconjugation
Drug Modfication Conjugation
PEGylation
Dextran Conjugation
Macrocyclics Metal Chelators
Dendritic Bioconjugation
Luminex Beads
Gold Nanoparticles
Micro and Nano Particles
Small Molecule Bioconjugation

Service by Application

Diagnostic Services

Biopharmaceutical Services




 
Oligo Nucleic Acid Bioconjugation
 
Oligo Nucleic Acid Bioconjugation

Oligo Nucleic Acid Modifications and Bioconjugations

Bio-Synthesis offers custom nucleic acid and oligonucleotide bioconjugation reagents as highly sensitive detection tools for customers to assaying oligonucleotide interaction or as therapeutic agents. Our nucleic acid and oligonucleotide conjugation services offer chemical modification of nucleic acid at specific sites within individual nucleotides or within oligonucleotides which allows labels such as fluorescence, chemiluminescence or chromogenic enzyme substrates, as well as small and macromolecules to be incorporated into DNA, RNA, BNA or PNA probes or immobilized on the surface to facilitate diagnostic and targeted drug delivery.

Bio-Synthesis gives you the best quality in nucleic acid chemistry industry by implementing a state-of-the art gene synthesis platform and expertise in providing high quality nucleic acid bioconjugate reagents. Nucleic acid and oligonucleotide modification and conjugates produced at Bio-Synthesis have substantial purity. Bio-Synthesis is committed to Total Quality Management (TQM) to assure customers' complete satisfaction. Each oligo-biopolymer conjugate is meticulously monitored during synthesis and controlled according to Bio-Synthesis' stringent quality assurance and quality control standards. The final product is identified by mass spectrum and purity is analyzed by high throughput gel electrophoresis or analytical HPLC or any other appropriate QC methods. QA (quality assurance) procedures are also followed independently to double guarantee the high quality of every delivered peptide. Bio-Synthesis's Total Quality Management System(TQM) has been successfully upgraded to fully comply with ISO 9001:2008 regulations.

Custom Oligo Conjugation Services

Bio-Synthesis, the leader in providing oligonucleotide and gene synthesis since 1984, provides affordable custom nucleic acids, oligos or oligomimetic-biomolecule hybrid conjugates by providing our clients with comprehensive modifications and labeling to be used in  biology, diagnostic, and drug discovery.

We offer enzymatic labeling of DNA as well as chemical modification of nucleic acid and oligonucleotides. These chemically modified oligonucleotides are extremely useful in fixing conformations by introducing cross-linkers in DNA, RNA, or nucleic acid-biomolecule complexes. Site-specific cross-linking permits the determination of the proximity of nucleotides or amino acids because the cross-linking woud not be possible at distances greater than the length of the spacer.  Such reagents are usually attached to either the base or the sugar moiety in most cases.

For the last two decades, we have accumulated a portfolio of oligonucleotide bioconjugate. Contact our National Customer Service Center at 800.220.0627 or contact us online with your detailed project descriptions,  in most case, we can accommodate your bioconjugation needs!

Service Portfolios

  • Oligonucleotide-enzyme conjugates for diagnostic assay
  • DNA, small RNA, siRNA polyethylenimine (PEI) conjugates
  • Biotin-oligo labeling for immunoassay
  • Oligonucleotide-nanoparticle conjugates
  • RNA-antibody conjugates  for immunoassay
  • DNA-antibody conjugates for immuno PCR
  • DNA, RNA-Protein conjugates to study protein to protein interaction
  • siRNA-peptide conjugates for siRNA delivery
  • PNA-siRNA conjugates for therapeutic drug discovery
  • PNA-DNA conjugates for gene inhibition study
  • DNA-quantum dot conjuguates for high sensitive detection application
  • DNA-KLH conjugates for antibody production
  • Oligonucleotide-agarose conjugates affinity chromatography immobilization
  • Oligonucleotide-drug conjugates for drug delivery
  • Conjugation of Genomic DNA to antibody
  • Coupling of metal chelates onto recombinant proteins and antibodies (including the difficult IgMs) for radiolabeling
  • DNA-lipid conjugates for cellular uptake
  • Oligonucleotide-bead conjuguates for luminex assay
  • DNA-glass plate conjuguate for microarray detection
  • Nucleic acid photoreactive conjugates for nucleic acid-protein interaction
  • Polyethylenimine bioconjugtes for imaging and DNA delivery in vivo
  • Site-Specific DNA labeling by Staudinger Ligation or Click Chemistry
  • Antisense peptide nucleic acid for improving cellular uptake
  • Oligonucleotide-peptide conjugates for biomedical and technological applications
  • Nucleic acid-polymer hybrid conjugates for diagnostic and biomedicine

Oligonucleotide Bioconjugation Service Descriptions

Chemistry: Using preactivated small molecule and biomolecule with chemical reactive groups such as amine, thiol, carboxylate, hydroxyl, aldehyde and ketone, active hydrogen, photo-chemical and ccloadition reactions and  cross link via zero-length , homobifunctional, heterobiofunctional  or multifunctioanl cross-linking chemistries, denrimer and dendrons, cleavable regent system.

Specification:  After standard desalting, or purification, a small percent of heterogeneous products containing single or multi-site conjugate per molecule may exist.

Material:

  • Nucleic Acids and Oligonucleotides: DNA, RNA, siRNA, Peptide Nucleic Acid (PNA), DNA mimetic, RNA mimetics
  • Biopolymers
    • Protein: Enzyme, antibodies, antigens, cell adhesion molecules
    • Peptides: Synthetic polypeptides
    • Saccharides:  Sugars, oligosaccharides and polysaccharides
    • Lipids:  Fatty acids, phospholipids, glycolipids and any fat-like substances.
    • Ligands:  Hormone receptors, cell surface receptors, avidin and biotin, small molecules
    • Labels: Fluorescent dyes, infrared-absorbing and UV-Vis absorption chromophores, nonradioactive labels
    • Nucleic acids and nucleotides: DNA, RNA, PNA,  nucleic acid analogs and genomic DNA
    • Synthetic polymers: PEG, Nanoparticles, gold particles, dendrimers, dendron, PAMAM
    • Others:  Conjugated or mixtures of any the above
    • Solid Supports: agarose, glass plates, membrane, beads

Procedure:  All custom synthesis of biomolecule, modification or bioconjugation services are manufactured under strict quality control processes. Analytical HPLC and MS analyses are performed in every development cycle. Final target conjugates must first be isolated from excess or unreacted reagent. In many cases, simple dialysis may suffice to remove unreacted reagent from the reaction solution.  Depending on the project scope, size-exclusion chromatography (SEC), HPLC,  may also be used to either remove excess reagent or isolate and characterized the cross-linked product. Cross-linked target molecule may then be further characterized by biochemical or biophysical techniques. Once the product has been purified, it may be subject to many different types of studies including spectroscopic (MALDI-TOF, ESI, LC-MS Fluorescence), electrophoresis, immunochemical biochemical, enzymatical analysis.  QC (quality control) and QA (quality assurance) procedures are also followed independently to offer you double guarantee for the highest quality possible of every delivered conjugates. Moreover, our dedicated technical account managers will guide your project through every step of the process and constantly keep you informed of the latest project progress.

Delivery Specifications:  The typical delivery consists of lyophilized sample in individual fully labeled vials. The shipment also contains COA, MS, HPLC and/or other analytical data.  Additional analytical data is also available upon request.

This service is for oligonucleotide bioconjugation using various types of crosslinking chemistries. See detailed on starting material provided by customer. If you can't find what you want? Please contact us online with your detail project descriptions, in most case, we can accommodate your bioconjugation needs!

Price: The price varies based on the project specifications. Our service includes materials and labor for conjugation only! Price does not include the cost of biopolymer synthesis and, if deemed necessary, biopolymer modification to introduce additional functional groups, extra linkers, spacers. Please contact us for a quote.

Oligo Nucleic Acid Bioconjugation Catalog No.
Antibody: DNA-Antibody Conjugation BIOCON30000
Antibody: DNA-Half Antibody Conjugation BIOCON30001
Antibody: dsDNA-Antibody Conjugation BIOCON30002
Antibody: dsDNA-Half Antibody Conjugation BIOCON30003
Basic Biopolymer Conjugation BIOCON30004
Enzyme Conjugation: DNA-AP Conjugates BIOCON30005
Enzyme Conjugation: DNA-HRP Conjugates BIOCON30006
Enzyme Conjugation: Oligo-Enzyme Conjugates BIOCON30007
Fatty Acid: DNA-Fatty Acid Conjugation BIOCON30008
Fatty Acid: Oligo-Lipids Conjugates BIOCON30009
Glycomimetic Oligo Conjugates BIOCON30010
Hapten: Oligo-BSA Conjugates BIOCON30011
Hapten: Oligo-Carrier Conjugation BIOCON30012
Hapten: DNA-KLH Conjugates BIOCON30013
Hapten: Oligo-Toxin Conjugates BIOCON30014
Metal Chelates: 2,2’-Dipicolylamine Oligo Conjugates BIOCON30015
Metal Chelates: DOTA Oligo Conjugates BIOCON30016
Metal Chelates: DTPA Oligo Conjugates BIOCON30017
Metal Chelates: NOTA Oligo Conjugates BIOCON30018
Metal Chelates: TETA Oligo Conjugates BIOCON30019
Oligo-Synthetic Polymer Conjugation BIOCON30020
Peptide: DNA-Peptide Conjugation BIOCON30021
Peptide: PNA-Peptide Conjugation (user supplied PNA material) BIOCON30022
Peptide: RNA Peptide Conjugation BIOCON30023
Peptide: siRNA Peptide Conjugation BIOCON30024
Small Molecule: DNA-Drug Conjugation BIOCON30025
Small Molecule: DNA-Small Molecule Conjugates BIOCON30026
Small Molecule: PNA-Drug Conjugation (user supplied PNA material) BIOCON30027
Small Molecule: PNA-Small Molecule Conjugates (user supplied PNA material) BIOCON30028
Small Molecule: RNA-Drug Conjugation BIOCON30029
Small Molecule: RNA-Small Molecule Conjugates BIOCON30030
Oligo Nucleic Acid Labeling Catalog No.
Oligo Nucleic Acid Immobilization Catalog No.
Oligo Nucleic Acid Modifications Catalog No.

Links and Resources

Reference/Citing:

  1. Upadhyay, A. et al.: Immunological Response to Peptide Nucleic Acid and its Peptide Conjugate Targeted to Transactivation Response (TAR) Region of HIV-1 RNA Genome; Oligonucleotides. 18(4) 2008.
  2. Olejnik, J. et al.: Photocleavable peptide-DNA conjugates: synthesis and applications to DNA analysis using MALDI-MS; Nucleic Acid Researech. 27 (23) 1999.
  3. Pai, S. et al.: Proximity ligation assays with peptide conjugate 'burrs' for the sensitive detection of spores; Nucleic Acid Research. 33(18) 2005.

Visit our literature vaults for more references and citings.

Ordering and submitting a request for Bioconjugation Services

For us to better understand your customized project, please complete our Bioconjugation Service Questionnaire. The more our chemists understand your project needs, the more accurate feedback we will be able to provide you.  Providing us with your project details will enable us to recommend the best reagents to use for your own project.  The most useful and readily available tools for bioconjugation projects are cross-linking reagents. A large number of cross-linkers, also known as bifunctional reagents, have been developed.  There are several ways to classify the cross-linkers, such as the type of reactive group, hydrophobicity or hydrophilicity, and the length of the spacer between reactive groups.  Other factors to consider are whether the two reactive groups are the same or different (for example, heterobifunctional or homobifunctional reagents), whether the spacer is cleavable, and whether the reagents are membrane permeable or impermeable.  The most accessible and abundant reactive groups in proteins are the ϵ-amino groups of lysine.  Therefore, a large number of the most common cross-linkers are amino selective reagents, such as imidoesters, sulfo-N-hydroxysuccinimide esters, and N-hydroxysuccinimide esters.  Due to the high reactivity of the thiol group with N-ethylmaleimide, iodoacetate and a-halocarbonyl compounds, new cross-linkers have been developed that contain maleimide and a-carbonyl moieties.  Usually, N-alkylmaleimides are more stable than their N-aryl counterparts.

 

In addition to the reactive groups on the cross-linkers, a wide variety of connectors and spacer arms have also been developed.  The nature of the spacer arm, and also the length, play an important role in the functionality.  Longer spacer arms are generally more effective when coupling large proteins or those with sterically protected reactive side-chains.  Other important considerations are the hydrophobicity, hydrophilicity, and the conformational flexibility.  Long aliphatic chains generally fold on themselves when in an aqueous environment, which makes the actual distance spanned by such linker arms less than expected.  Instead, spacers that contain more rigid structures (for example, aromatic groups or cycloalkanes) should be used.  These structures, however, tend to be very hydrophobic which could significantly decrease the solubility of the modified molecules or even modify some of their properties.  In such cases, it is recommended to choose a spacer that contains an alkylether (PEO) chain.  Bio-Synthesis offers several cross-linkers with PEO chains, such as thiol-binding homobifunctional reagents, heterobifunctional based, and their derivatives.

Once the project scope has collected, we will provide an appropriate quotation within 3-5 days. Orders can be placed with either a PO (Purchase Order) or credit card. We accept POs and major credit cards ( ). Your credit card will be billed under 'Bio-Synthesis, Inc.' Click here to download our credit reference form. For international orders, we must apply the full charge at the time of the order is placed. In the unlikely event that any given order cannot be filled, our guarantee will take the form of a full refund.